• 专利标题:   Preparing modified graphene used for lubricating mechanical structures, by adding graphene, processing, melting, dripping surface modifier, refluxing, subjecting graphene to addition reaction with surface modifier and purifying graphene.
  • 专利号:   CN110387282-A
  • 发明人:   FENG W, ZHANG Y, GUO S, ZHANG C, ZHANG S
  • 专利权人:   SHENZHEN INST ADVANCED TECHNOLOGY
  • 国际专利分类:   C01B032/194, C10M141/02, C10M159/12, C10N030/02, C10N030/06, C10N030/12
  • 专利详细信息:   CN110387282-A 29 Oct 2019 C10M-159/12 201988 Pages: 12 Chinese
  • 申请详细信息:   CN110387282-A CN10617019 09 Jul 2019
  • 优先权号:   CN10617019

▎ 摘  要

NOVELTY - Method for preparing modified graphene, involves (i) providing graphene with an unsaturated carbon six-membered ring, adding the graphene to a reaction kettle and ultrasonically processing the graphene, and (ii) completely melting the graphene, dripping a surface modifier in the reaction kettle, refluxing, subjecting the graphene to addition reaction with the surface modifier, so that the unsaturated carbon six-membered ring is connected with a long-chain carboxyl group having 8-22C, and purifying to obtain the finished product. The surface modifier comprises a first carboxyl compound and a second carboxyl compound. USE - The modified graphene is used in lubricating oil for lubricating mechanical structures (all claimed). ADVANTAGE - The modified graphene improves the dispersibility of graphene in an oily solvent. DETAILED DESCRIPTION - INDEPENDENT CLAIMS are included for the following: (1) a modified graphene comprising a graphene having an unsaturated carbon six-membered ring, where the unsaturated carbon six-membered ring has a long-chain carboxyl group having 8-22C; and (2) a lubricating oil comprising a base oil, and 0.04-0.08 %mass modified graphene, which is uniformly dispersed in the base oil.