• 专利标题:   Preparation of reduced graphene oxide by grinding carbon rods in waste zinc-manganese battery, mixing carbon rod powder and sodium hydroxide, melting, mixing water, peeling off zinc skin shell of waste zinc manganese battery, and reacting.
  • 专利号:   CN112250062-A, CN112250062-B
  • 发明人:   YANG M, LIU J
  • 专利权人:   UNIV WUHAN POLYTECHNIC
  • 国际专利分类:   C01B032/184
  • 专利详细信息:   CN112250062-A 22 Jan 2021 C01B-032/184 202121 Pages: 10 Chinese
  • 申请详细信息:   CN112250062-A CN11111021 16 Oct 2020
  • 优先权号:   CN11111021

▎ 摘  要

NOVELTY - Preparation of reduced graphene oxide comprises cleaning, drying, grinding and sieving carbon rods in waste zinc-manganese battery to obtain carbon rod powder; mixing carbon rod powder and sodium hydroxide, melting and cooling to obtain cooled alkali fusion sample; mixing cooled alkali-melted sample with water, filtering to obtain filter residue, and reacting filter residue with hydrochloric acid to obtain purified graphite powder; washing, drying, grinding and sieving solid manganese oxide in waste zinc-manganese battery to get manganese oxide powder; peeling off zinc skin shell of waste zinc manganese battery, washing and cutting to obtain zinc flakes; and performing contact reaction of purified graphite powder, manganese oxide powder, potassium sulfate and sulfuric acid, and adding water and zinc flakes to continue reacting. USE - The method is used for preparing reduced graphene oxide (claimed). ADVANTAGE - The method firstly uses material in waste zinc-manganese battery to prepare reducing graphene oxide, which not only solves processing problem of waste battery.