• 专利标题:   Preparing composite material involves oxidizing grafite by ultrasonic wave to obtain oxidized graphite alkene solution, which is mixed with polyethylenimine solution to obtain graphene oxide and polyethylenimine solution mixture.
  • 专利号:   CN104759268-A, CN104759268-B
  • 发明人:   WANG L, ZHAO C
  • 专利权人:   UNIV CHANGSHA
  • 国际专利分类:   B01J020/26, B01J020/28, B01J020/30
  • 专利详细信息:   CN104759268-A 08 Jul 2015 B01J-020/26 201573 Pages: 7 Chinese
  • 申请详细信息:   CN104759268-A CN10177430 15 Apr 2015
  • 优先权号:   CN10177430

▎ 摘  要

NOVELTY - Preparing composite material involves oxidizing grafite by ultrasonic wave to obtain oxidized graphite alkene solution (1-8mg/mL). The obtained oxidized graphite alkene solution and polyethylenimine solution (5-40mg/mL) are mixed in ratio of 1:0.3-3 to obtain graphene oxide and polyethylenimine solution mixture by crosslinking reaction. Activated carbon fiber (5-10g) is dipped with concentrated nitric acid (500mL) and sonicated. Deionized water is removed from the mixture and pH is adjusted to 5-6. The mixture is dried at 70-80 degrees C. USE - Method for preparing composite material (claimed). ADVANTAGE - The method enables to prepare composite material in simple and eco-friendly manner. DETAILED DESCRIPTION - Preparing composite material involves oxidizing grafite by ultrasonic wave to obtain oxidized graphite alkene solution (1-8mg/mL). The obtained oxidized graphite alkene solution and polyethylenimine solution (5-40mg/mL) are mixed in ratio of 1:0.3-3 to obtain graphene oxide and polyethylenimine solution mixture by crosslinking reaction. Activated carbon fiber (5-10g) is dipped with concentrated nitric acid (500mL) and sonicated. Deionized water is removed from the mixture and pH is adjusted to 5-6. The mixture is dried at 70-80 degrees C. The obtained pre-impregnated activated carbon fiber is mixed with obtained graphene oxide and polyethylenimine solution mixture and dried at 70-80 degrees C. Surface area of the obtained composites is 1400-1600m2/g. The composite material has pore diameter 1-4.5nm and pore size of 0.5-2nm.