• 专利标题:   Preparation of carbon-coated manganese oxide/nitrogen-doped reduced graphene oxide lithium ion battery cathode material involves dissolving manganese acetate in water, adding graphene oxide to manganese acetate solution and stirring.
  • 专利号:   CN107123794-A
  • 发明人:   CAO L, WANG R, XU Z, LI J, HUANG J, LI R, LI K
  • 专利权人:   UNIV SHAANXI SCI TECHNOLOGY
  • 国际专利分类:   H01M010/0525, H01M004/36, H01M004/50, H01M004/62
  • 专利详细信息:   CN107123794-A 01 Sep 2017 H01M-004/36 201776 Pages: 8 Chinese
  • 申请详细信息:   CN107123794-A CN10318940 08 May 2017
  • 优先权号:   CN10318940

▎ 摘  要

NOVELTY - The preparation method of carbon-coated manganese oxide/nitrogen-doped reduced graphene oxide lithium ion battery cathode material involves dissolving manganese acetate in water and evenly mixing to prepare manganese acetate solution, adding graphene oxide to the manganese acetate solution, stirring and ultrasonically dispersing the mixture, transferring the mixture to reaction kettle and carrying out microwave hydrothermal reaction, mixing microwave hydrothermal reaction product with sucrose and transferring to PTFE reactor, filtering, washing and drying. USE - The method is useful for preparing carbon-coated manganese oxide/nitrogen-doped reduced graphene oxide lithium ion battery cathode material (claimed). ADVANTAGE - The method enables preparation of carbon-coated manganese oxide/nitrogen-doped reduced graphene oxide lithium ion battery cathode material with excellent circulation stability. DETAILED DESCRIPTION - The preparation method of carbon-coated manganese oxide/nitrogen-doped reduced graphene oxide lithium ion battery cathode material involves dissolving manganese acetate in water and evenly mixing at room temperature to prepare 2.5-8.5 %mass manganese acetate solution, adding 30-100 mg graphene oxide to the 40-70 ml manganese acetate solution, stirring and ultrasonically dispersing the mixture, transferring the mixture to reaction kettle and carrying out microwave hydrothermal reaction, mixing microwave hydrothermal reaction product with 1.2-3.5 g sucrose and transferring to PTFE reactor, filtering, washing and drying hydrothermal reaction product, heat-treating product in an atmosphere furnace to obtain solid particles having particle size of 100 nm, and coating granular manganese oxide surface with uniform carbon layer.