• 专利标题:   Graphene composite oxide modified attapulgite water purifying agent comprises graphene oxide, attapulgite, hexadecyl trimethyl ammonium bromide, dodecyl benzene sulfonic acid, polyaniline, diluted hydrochloric acid and de-ionized water.
  • 专利号:   CN108686633-A
  • 发明人:   CHE C
  • 专利权人:   JINAN DEV ZONE XINGHUO TECHNOLOGY RES
  • 国际专利分类:   B01J020/26, C02F001/28, B01J020/30, C02F101/20
  • 专利详细信息:   CN108686633-A 23 Oct 2018 B01J-020/26 201901 Pages: 5 Chinese
  • 申请详细信息:   CN108686633-A CN10751108 10 Jul 2018
  • 优先权号:   CN10751108

▎ 摘  要

NOVELTY - Graphene composite oxide modified attapulgite water purifying agent comprises 10-15 pts. wt. graphene oxide, 20-35 pts. wt. attapulgite, 2-5 pts. wt. hexadecyl trimethyl ammonium bromide, 1-3 pts. wt. dodecyl benzene sulfonic acid, 5-12 pts. wt. calcium powder, 5-10 pts. wt. polyvinyl alcohol, 3-8 pts. wt. polyaniline, diluted hydrochloric acid and de-ionized water. USE - Graphene composite oxide modified attapulgite water purifying agent. ADVANTAGE - The graphene composite oxide modified attapulgite water purifying agent is eco-friendly, has super large specific surface area and good water purifying effect. DETAILED DESCRIPTION - An INDEPENDENT CLAIM is included for a method for preparing graphene composite oxide modified attapulgite water purifying agent, which involves: (A) adding attapulgite into deionized water, stirring for 30-60 minutes to disperse uniformly, adding hexadecyltrimethyl ammonium bromide and stirring for 8-10 hours, filtering and drying attapulgite to obtain modified; (B) adding modified attapulgite into deionized water, stirring and dispersing ultrasonically for 30-60 minutes to obtain modified attapulgite dispersion; (C) adding oxidized graphene into de-ionized water, performing ultrasonic treatment for 30-60 minutes, forming uniformly dispersed graphene oxide dispersing liquid; (D) mixing polyvinyl alcohol, mixing polyaniline solution into ultrasonic for 30 minutes to obtain mixed solution A in graphene oxide dispersion; (E) stirring modified attapulgite dispersion ultrasonically and mechanically, adding calcium aluminate powder, dodecyl benzene sulfonic acid, mixing ultrasonically, stirring mechanically for 2-3 hours; and (F) using diluted hydrochloric acid to adjust pH to 2, standing, washing by de-ionized water for three times and centrifuging to obtain precipitate, drying in vacuum and grinding into powder to obtain water purifying agent.