• 专利标题:   Enhancing low oxygen content graphene dispersibility by mixing graphene powder and water, sonicating, water bath heating, dropping silane coupling agent, and mixing modified graphene dispersion liquid, polyether macromonomer and initiator.
  • 专利号:   CN113184841-A
  • 发明人:   LIU Y, WU J, LUO S, LIU M, WANG D
  • 专利权人:   SHENZHEN GANGCHUANG BUILDING MATERIAL CO
  • 国际专利分类:   C01B032/194
  • 专利详细信息:   CN113184841-A 30 Jul 2021 C01B-032/194 202182 Pages: 6 Chinese
  • 申请详细信息:   CN113184841-A CN10543886 19 May 2021
  • 优先权号:   CN10543886

▎ 摘  要

NOVELTY - Enhancing low oxygen content graphene dispersibility comprises weighing 0.1-1 pts. wt. graphene powder, stirring with 90-99.9 pts. wt. deionized water, and dispersing under ultrasonic condition; putting processed dispersion in reaction kettle, stirring, and water bath heating to 60-80 degrees C; weighing 0.1-3 pts. wt. silane coupling agent, and adding into reaction kettle by dropping for 0.5-1.5 hours; mixing 40-60 pts. wt. modified graphene dispersion liquid, 20-30 pts. wt. polyether macromonomer and 0.1-1 pts. wt. initiator; putting in reaction kettle at 200-400 revolutions/minute; weighing 2-6 pts. wt. acrylic acid or methacrylic acid and 1-3 pts. wt. p-styrene sulfonic acid sodium, and weighing 2-6 pts. wt. water to prepare liquid; weighing 0.1-1 wt.% reducing agent and 0.1-1 wt.% chain transfer agent to prepare second solution; and stirring uniformly, dropping, dripping for 2-3.5 hours, and replenishing water to reaction system. USE - The method is used for enhancing low oxygen content graphene dispersibility. ADVANTAGE - The method has mild reaction condition, and does not need or only needs small amount of organic solvent. The device requirement is not high. It can solve dispersion problem of graphene, and reduce dispersion cost.