• 专利标题:   Rapid preparation of supramolecular cyclodextrin metal-organic framework and graphene composite used in adsorption treatment of organic dyes, by dissolving cyclodextrin, potassium hydroxide and nucleating agent graphene in deionized water, allowing to stand, washing with methanol, and drying.
  • 专利号:   CN116099508-A
  • 发明人:   XIA T, LI X, ZHENG Z, ZHANG W
  • 专利权人:   UNIV YANGZHOU
  • 国际专利分类:   B01J020/24, B01J020/30, C02F001/28, C02F101/30, C08G083/00
  • 专利详细信息:   CN116099508-A 12 May 2023 B01J-020/24 202349 Chinese
  • 申请详细信息:   CN116099508-A CN11662121 23 Dec 2022
  • 优先权号:   CN11662121

▎ 摘  要

NOVELTY - Rapid preparation of supramolecular cyclodextrin metal-organic framework and graphene composite comprises dissolving cyclodextrin, potassium hydroxide and nucleating agent graphene in deionized water, stirring quickly with a mixer to make it fully mixed, adding methanol as a reaction solvent during the stirring process, adding the mixed solution into a microwave reactor, taking out after microwave reaction, pouring it into a methanol solution to induce the growth of a gray crystal cyclodextrin metal organic framework, allowing to stand, washing it with methanol, and fully drying to obtain the final product supramolecular cyclodextrin metal organic framework and graphene composite. USE - The method is useful for rapid preparation of supramolecular cyclodextrin metal-organic framework and graphene composite. ADVANTAGE - The method makes full use of the characteristics of microwave rapid crystal synthesis and graphene providing nucleation sites, and completes the reaction within a few minutes, fully solves the long-time problem of preparing cyclodextrin metal-organic frameworks and has very broad application prospects. DETAILED DESCRIPTION - An INDEPENDENT CLAIM is also included for a use method of a supramolecular cyclodextrin metal organic framework and a graphene composite material for adsorption comprising providing the supramolecular cyclodextrin metal organic framework and graphene composite material, adding it to the methanol solution of organic dyes at room temperature, and allowing to stand for a certain period of time for adsorption.