• 专利标题:   Improved method for preparation of graphene oxide from natural graphite in modified dual drive planetary ball mill, involves peeling or de-laminating graphite powder / flake occurred during milling process inside dual drive high energy planetary ball mill.
  • 专利号:   IN201400763-I2
  • 发明人:   ROUT T K, DAS S, SAHU A K, DASH P, BISWAL S K, MISRA B K
  • 专利权人:   TATA STEEL LTD, COUNCIL SCI IND RES INDIA
  • 国际专利分类:   B02C017/08
  • 专利详细信息:   IN201400763-I2 17 Sep 2021 B02C-017/08 202181 Pages: 26 English
  • 申请详细信息:   IN201400763-I2 INKO00763 16 Jul 2014
  • 优先权号:   INKO00763

▎ 摘  要

NOVELTY - The method involves feeding natural graphite of more than 99% purity into a dual drive high energy planetary ball mill (3) in a dry method. A solid state oxidizing reaction is allowed to graphite in the dual drive high energy planetary ball mill. The oxidizing of graphite powder occurs inside the jars of the high enery gall mill and peeling of or de-lamination of graphite powder / flake occurred during the milling process inside the dual drive high energy planetary ball mill are performed. The graphite particles size varies in the range of 600 micron to 5 micron. The graphene oxide is comprised of ten stacking layers. USE - Improved method for preparation of graphene oxide from natural graphite in modified dual drive planetary ball mill. ADVANTAGE - The improved process for preparation of graphene oxide from natural graphite in a modified dual drive planetary ball mill in which the shearing action of the balls in a dual drive vertical swing planetary ball mill is made use, chemicals and acids are not used, and process is performed in single step operation. The environmental friendly process is achieved with zero waste. DESCRIPTION OF DRAWING(S) - The drawing shows a schematic view showing the improved process for preparation of graphene oxide from natural graphite in modified dual drive planetary ball mill. Structural frame (1) Rotating arm (2) Ball mill (3) Pulley arrangement (4) Gyro pulley (5)