• 专利标题:   Preparation of graphene-silver nanoparticle composite film for ultraviolet detector includes mixing graphene oxide hydrazine hydrate in de-ionized water, reacting, adding soluble silver salt and sodium citrate, reducing and centrifuging.
  • 专利号:   CN106346016-A, CN106346016-B
  • 发明人:   LIN Y, YAO G, ZHANG H
  • 专利权人:   UNIV CHINA ELECTRONIC SCI TECHNOLOGY
  • 国际专利分类:   B05D001/00, B22F009/24, B82Y040/00, G01J001/42
  • 专利详细信息:   CN106346016-A 25 Jan 2017 B22F-009/24 201719 Pages: 12 Chinese
  • 申请详细信息:   CN106346016-A CN10763647 30 Aug 2016
  • 优先权号:   CN10763647

▎ 摘  要

NOVELTY - Preparation of graphene-silver nanoparticle composite film includes mixing the graphene oxide and hydrazine hydrate in de-ionized water to obtain dispersion, adding soluble silver salt and sodium citrate, reduction to obtain graphene-silver nanoparticle composite solution, centrifuging, washing in de-ionized water, removing excess reducing agent and free silver nanoparticles on the substrate and drying. USE - Preparation of graphene-silver nanoparticle composite film for ultraviolet detector. ADVANTAGE - Graphene based silver nanoparticle composite film has larger photocurrent from ultraviolet light, thus lessening recovery time. DETAILED DESCRIPTION - Preparation of graphene-silver nanoparticle composite film comprises ultrasonic mixing the graphene oxide and hydrazine hydrate in de-ionized water to obtain dispersion where graphene oxide and hydrazine hydrate ratio is 1:10-40, oxidized graphene at 0.3-0.6 g/L, reacting for 24-48 hours in a 100 degrees C oil bath, adding soluble silver salt and sodium citrate, adding deionized water, ultrasonic mixing, adding soluble silver salt and sodium citrate at a ratio of 50-100:1 where the concentration of soluble silver salt is 0.02-0.05 mol/L, uniformly mixing, ultrasonic stirring and reacting for 1 to 2 hours, reduction to obtain graphene-silver nanoparticle composite solution, centrifuging, washing in de-ionized water, removing excess reducing agent and free silver nanoparticles on the substrate and drying. DESCRIPTION OF DRAWING(S) - The drawing is a flowchart of the preparation of graphene-silver nanoparticle composite film (Drawing includes non-English language text).