• 专利标题:   Preparation of graphene composite sponge involves washing discarded cigarette ends, drying, immersing in graphene oxide solution, drying, heating, washing natural cotton, mixing with urea solution, freeze-drying and heating.
  • 专利号:   CN110627044-A
  • 发明人:   SHI J
  • 专利权人:   SHI J
  • 国际专利分类:   C01B032/184, C01B032/194, C01B032/198, D01F009/16
  • 专利详细信息:   CN110627044-A 31 Dec 2019 C01B-032/184 202010 Pages: 7 Chinese
  • 申请详细信息:   CN110627044-A CN10649014 22 Jun 2018
  • 优先权号:   CN10649014

▎ 摘  要

NOVELTY - Preparation of graphene composite sponge involves preparing experimental materials and instruments, washing discarded cigarette ends, drying, immersing in a graphene oxide solution, drying, heating in a tube furnace at 900 degrees C at rate of 5 degrees C/minute for two hours, washing and drying natural cotton, mixing with urea solution in a mold, freeze-drying to obtain cotton-urea block, heating the block at 600 degrees C at rate of 1 degrees C/minute in a tube furnace for 1 hour, increasing the temperature to 900 degrees C, cooling to room temperature to obtain nitrogen doped graphene-carbon fiber composite sponge, mixing graphene oxide and graphene oxide nanoribbons in mass ratio of 1:1 with deionized water, adding the solution to a beaker, freezing for more than 24 hours, vacuum freeze-drying for 48 hours, removing the composite sponge from the mold, and reducing in hydrazine hydrate steam at 90 degrees C for 24 hours to obtain a graphene-graphene nanoribbon composite sponge, and comparing the preparing composite sponges. USE - Preparation of graphene composite sponge. ADVANTAGE - The graphene composite sponge having excellent strength can be produced.