• 专利标题:   Preparation of glass fiber ball bundle loaded graphene aerogel, by adding graphene oxide to dispersant, ultrasonically processing, taking upper dispersion, adding ethylenediamine, ultrasonically processing, adding glass fiber ball bundles, stirring, filtering, collecting sample, and vacuum-drying.
  • 专利号:   CN116078294-A
  • 发明人:   LIN J, GUAN C
  • 专利权人:   UNIV SHANGHAI POLYTECHNIC
  • 国际专利分类:   B01J013/00
  • 专利详细信息:   CN116078294-A 09 May 2023 B01J-013/00 202347 Chinese
  • 申请详细信息:   CN116078294-A CN10038602 13 Jan 2023
  • 优先权号:   CN10038602

▎ 摘  要

NOVELTY - Preparation of glass fiber ball bundle loaded graphene aerogel involves (1) preparing glass fiber ball bundles using waste printed circuit board non-metallic powder, and immersing in 0.1-3 wt.% hydrofluoric acid aqueous solution for 3-30 minutes, (2) adding graphene oxide to dispersant, ultrasonically processing for 10-60 minutes, taking upper dispersion, adding ethylenediamine, ultrasonically processing again for 10-60 minutes, then adding the glass fiber ball bundles, stirring for 5-30 minutes, filtering through an 80-100 mesh screen, washing with washing liquid, and collecting a glass fiber bundle sample, (3) freezing the sample under liquid nitrogen for 5-10 minutes, and freeze-drying at 30-100℃ for 12-24 hours to obtain glass fiber ball bundle-loaded graphene oxide aerogel, and (4) vacuum-drying at 100-200℃ for 12-24 hours. USE - Preparation of glass fiber ball bundle loaded graphene aerogel (claimed). ADVANTAGE - The method provides glass fiber ball bundle loaded graphene aerogel, which is convenient to use, has wide application range, and makes up for the deficiency of block-shaped aerogel.