• 专利标题:   Preparing photocatalytic acarus-removing antibacterial disinfectant, comprises e.g. adding titanium trichloride to deionized water, ultrasonically dispersing, adding hydrochloric acid, continuously performing ultrasonic dispersion, centrifuging, washing, drying, calcining, and adding graphene oxide.
  • 专利号:   CN114009456-A, CN114009456-B
  • 发明人:   TANG G, CHAI C, GUO H, LIU H, ZHAN X, HE X, CUI H
  • 专利权人:   UNIV HUAINAN UNION
  • 国际专利分类:   A01N059/00, A01N059/16, A01N065/12, A01P001/00, A01P003/00, A01P007/02
  • 专利详细信息:   CN114009456-A 08 Feb 2022 A01N-065/12 202238 Chinese
  • 申请详细信息:   CN114009456-A CN11301634 04 Nov 2021
  • 优先权号:   CN11301634

▎ 摘  要

NOVELTY - Preparing photocatalytic acarus-removing antibacterial disinfectant, comprises e.g. (i) adding titanium trichloride to deionized water, ultrasonically dispersing for 1-2 hours, adding hydrochloric acid in ultrasonic dispersion process, continuously performing ultrasonic dispersion for 1-2 hours, adding sodium metavanadate, stirring at 150-200degrees Celsius for 20-40 minutes, centrifuging, washing, drying, and calcining at 150-200degrees Celsius for 10-20 minutes to obtain nano-powder, (ii) adding the nano-powder into sodium hydroxide solution and stirring performing hydrothermal reaction at 150-200degrees Celsius for 10-20 hours, washing hydrothermal reaction product to neutrality, performing acid washed, drying, and performing heat treatment at 300-400degrees Celsius for 1-2 hours under argon protection to obtain composite nano-titanium dioxide powder, and (iii) adding graphene oxide in ethanol aqueous solution, performing ultrasonic dispersion for 1-2 hours, and adding composite nano-titanium dioxide powder. USE - The method is useful for preparing photocatalytic acarus-removing antibacterial disinfectant (claimed). DETAILED DESCRIPTION - Preparing photocatalytic acarus-removing antibacterial disinfectant, comprises (i) adding titanium trichloride to deionized water, ultrasonically dispersing for 1-2 hours at an ultrasonic power of 300-500 W, adding hydrochloric acid in the ultrasonic dispersion process, continuously performing ultrasonic dispersion for 1-2 hours, adding sodium metavanadate, stirring at 150-200degrees Celsius for 20-40 minutes, centrifuging, washing, drying, and calcining at 150-200degrees Celsius for 10-20 minutes to obtain nano-powder, (ii) adding the nano-powder into sodium hydroxide solution and stirring performing hydrothermal reaction at 150-200degrees Celsius for 10-20 hours, washing hydrothermal reaction product to neutrality, then performing acid washed, drying, and performing heat treatment at 300-400degrees Celsius for 1-2 hours under argon protection to obtain composite nano-titanium dioxide powder, and (iii) adding graphene oxide in the ethanol aqueous solution, performing ultrasonic dispersion for 1-2 hours, adding composite nano-titanium dioxide powder to disperse evenly, performing hydrothermal reaction at 140-180degrees Celsius for 20-30 hours, adding sodium dodecyl benzene sulfonate, cocoyl diethanolamine, fatty alcohol polyoxyethylene ether, fatty alcohol polyoxyethylene ether sodium sulfate, plant essential oil and water, and uniformly mixing to obtain a photocatalytic acarus-removing antibacterial disinfectant. An INDEPENDENT CLAIM is also included for photocatalytic acarus-removing antibacterial disinfectant prepared by the above-mentioned method.