• 专利标题:   Preparation of three-dimensional graphene oxide film ball modified organic composite ultra/microfiltration membrane involves mixing ethanol and water, adding graphene oxide powder, adding tetraethyl orthosilicate, and ultrasonic treating.
  • 专利号:   CN106582298-A
  • 发明人:   WANG L, ZHU Z, WANG X, LV Y, CHEN L, HUANG D, MIAO R, JIANG J, XU Y, LI Q, HUO X
  • 专利权人:   UNIV XIAN ARCHITECTURE TECHNOLOGY
  • 国际专利分类:   B01D067/00, B01D069/12, B01D071/30, B01D071/34, B01D071/42, B01D071/54, B01D071/68
  • 专利详细信息:   CN106582298-A 26 Apr 2017 B01D-067/00 201742 Pages: 7 Chinese
  • 申请详细信息:   CN106582298-A CN11130415 09 Dec 2016
  • 优先权号:   CN11130415

▎ 摘  要

NOVELTY - Preparation of three-dimensional graphene oxide film ball modified organic composite ultra/microfiltration membrane involves mixing 60-95 wt.% ethanol and water, adding 2-50 mg graphene oxide powder, adjusting pH to 8-9, adding 0.5-5 mg tetraethyl orthosilicate, ultrasonic treating, storing, centrifuging, washing, vacuum freeze-drying for 24 hours, mixing 0.1-1 wt.% graphene oxide particles to 70-80 wt.% organic solvent, ultrasonic treating, adding 1-5 wt.% polymer additives, mixing at 70 degrees C, dissolving, standing, defoaming for 10-15 hours, precipitating, and placing on clean glass plate. USE - Method for preparing three-dimensional graphene oxide film ball modified organic composite ultra/microfiltration membrane (claimed). ADVANTAGE - The material is non-polluting, high-strength, environment-friendly, and suitable for drinking water, food, and medicine. DETAILED DESCRIPTION - Preparation of three-dimensional graphene oxide film ball modified organic composite ultra/microfiltration membrane comprises mixing 60-95 wt.% ethanol and water, adding 2-50 mg graphene oxide powder, adjusting pH to 8-9, adding 0.5-5 mg tetraethyl orthosilicate, ultrasonic treating, storing, centrifuging, washing, vacuum freeze-drying for 24 hours, mixing 0.1-1 wt.% graphene oxide particles to 70-80 wt.% organic solvent, ultrasonic treating, adding 1-5 wt.% polymer additives, mixing at 70 degrees C, dissolving, standing, defoaming for 10-15 hours, precipitating, placing on clean glass plate, scraping, and soaking in deionized water for 24 hours.