• 专利标题:   Synthesizing porous graphene-type nanosheets using biomass as raw material comprises e.g. dissolving precursor in solvent and mixing to obtain precursor solution, magnetically stirring, cross-linking by heating and self-assembling, calcining mixture, washing sample in hydrochloric acid and drying.
  • 专利号:   CN115893384-A
  • 发明人:   ZHOU Y, LIANG Y, QI X
  • 专利权人:   UNIV NANKAI
  • 国际专利分类:   C01B032/184, C01B032/318, C01B032/348, H01G011/34, H01G011/44, H01G011/86
  • 专利详细信息:   CN115893384-A 04 Apr 2023 C01B-032/184 202337 Chinese
  • 申请详细信息:   CN115893384-A CN11498868 28 Nov 2022
  • 优先权号:   CN11498868

▎ 摘  要

NOVELTY - Synthesizing porous graphene-type nanosheets using biomass as raw material comprises e.g. dissolving precursor in solvent and mixing to obtain a precursor solution, dissolving 1 g non-ionic surfactant block copolymer F127 and ultrasonically assisting to dissolve in 30 ml solvent to prepare F127 solution, adding the precursor solution in dropwise to F127 solution and magnetically stirring the whole process, cross-linking by heating and self-assembling to form composite film, uniformly mixing cross-linked film material and activator into powder, cutting the obtained film into small pieces, gradually grinding ground with an activator in an agate mortar/or mixed into a powder by ball milling, calcining the mixture under a nitrogen atmosphere, washing sample in 2 M hydrochloric acid, and then washing repeatedly with ultrapure water until a neutral pH is obtained, and then drying at 80℃ for 12 hours, and denoting the obtained sample as gel permeation chromatography (GPC)-T. USE - The method is useful for synthesizing porous graphene-type nanosheets using biomass as raw material. ADVANTAGE - The method: is simple in synthesis process, safe, expandable and green, can prepare graphene nano sheet, which has high specific surface area, macroporous volume and hierarchical porous structure, and has good conductivity.