• 专利标题:   Water purification composite film material useful for removing heavy metal ions in the water, comprises titanium carbide and graphene.
  • 专利号:   CN107551829-A
  • 发明人:   XU Y, JIE X
  • 专利权人:   UNIV FUZHOU
  • 国际专利分类:   B01D067/00, B01D069/02, B01D069/12, B01D071/02, B01J020/20, B01J020/30, C02F001/28, C02F001/44, C02F101/20, C02F101/22
  • 专利详细信息:   CN107551829-A 09 Jan 2018 B01D-071/02 201810 Pages: 8 Chinese
  • 申请详细信息:   CN107551829-A CN11004590 25 Oct 2017
  • 优先权号:   CN11004590

▎ 摘  要

NOVELTY - Water purification composite film material comprises 80-95% titanium carbide and 5-20% graphene. The sum of the mass fraction of the two components is 100%. USE - The material is useful for removing heavy metal ions in the water (claimed). DETAILED DESCRIPTION - An INDEPENDENT CLAIM is also included for preparing water purification composite film material, comprising (i) adding titanium aluminum chloride into the lithium flouride hydrochloric acid solution, reacting at 35 degrees C for 24 hours, washing the resulting material with deionized water, re-dispersing in deionized water, ultrasonicating for 1 hour, centrifuging for 1 hour and taking the upper liquid to obtain titanium carbide nano-sheet colloidal solution; (ii) adding the polyethyleneimine solution into graphene oxide aqueous solution, refluxing at 90 degrees C for 2 hours, washing, centrifuging and re-dispersing the resulting graphene with deionized water to obtain graphene dispersion; (iii) adding the graphene dispersion into the titanium carbide nano sheet gel solution, stirring at room temperature for 1 hour and vacuum filtering; and (iv) immersing the composite membrane material n a hydrochloric acid solution for 24 hours and removing the excess hydrochloric acid using deionized water.