• 专利标题:   Biomass-based graphene quantum dot for e.g. illuminating anti-counterfeiting, is prepared by dissolving 2-aminobenzenesulfonic acid or para-toluenesulfonic acid in deionized water, heating, performing hydrothermal reaction, and dialyzing.
  • 专利号:   CN110257059-A
  • 发明人:   LI K, CHEN L, WANG R, ZHANG S, MIN Y, WANG H
  • 专利权人:   UNIV GUANGDONG TECHNOLOGY
  • 国际专利分类:   B82Y020/00, B82Y040/00, C09K011/65
  • 专利详细信息:   CN110257059-A 20 Sep 2019 C09K-011/65 201985 Pages: 6 Chinese
  • 申请详细信息:   CN110257059-A CN10548937 24 Jun 2019
  • 优先权号:   CN10548937

▎ 摘  要

NOVELTY - A biomass-based graphene quantum dot is prepared by dissolving 2-aminobenzenesulfonic acid or para-toluenesulfonic acid in deionized water, heating to 70-90 degrees C, stirring uniformly, adding alkali lignin, heat preserving at 70-90 degrees C, filtering the solution with aqueous filter membrane, collecting filtrate, adding alkali solution to filtrate for ultrasonically processing, and carrying out hydrothermal reaction at 180-220 degrees C, filtering using aqueous filter, collecting the filtrate, placing in cut-off dialysis bag, dialyzing with deionized water, and lyophilizing. USE - Biomass-based graphene quantum dot used for illuminating anti-counterfeiting (claimed), and in food and medicine. ADVANTAGE - The biomass-based graphene quantum dot prepared is simple, effective and economical, and does not require high temperature thermal cracking process. The preparation process is simple, safe and has short process flow. The biomass-based graphene quantum dots prepared have excellent biocompatibility, low biotoxicity and excellent photoluminescence properties. DETAILED DESCRIPTION - An INDEPENDENT CLAIM is included for preparation of biomass-based graphene quantum dot, which involves (1) dissolving 2-aminobenzenesulfonic acid or para-toluenesulfonic acid in deionized water, heating to 70-90 degrees C, stirring uniformly, adding alkali lignin, heat preserving at 70-90 degrees C, filtering the solution with aqueous filter membrane, collecting filtrate, adding alkali solution to filtrate for ultrasonically processing, and carrying out hydrothermal reaction at 180-220 degrees C to obtain solution (A), (2) and filtering solution (A) using aqueous filter, collecting the filtrate, placing in trapped dialysis bag, dialyzing with deionized water, and freeze-drying.