• 专利标题:   Preparation of water-soluble titanate coupling agent modified graphene for e.g. coatings, involves heating expandable graphite, oxidizing, adding titanate coupling agent and hydrazine hydrate, heating to react, filtering, and vacuum drying.
  • 专利号:   CN103342904-A
  • 发明人:   LI J, QIU H, YANG J, YANG Z
  • 专利权人:   UNIV SHANGHAI SCI TECHNOLOGY
  • 国际专利分类:   C09C001/46, C09C003/08
  • 专利详细信息:   CN103342904-A 09 Oct 2013 C09C-001/46 201403 Pages: 7 Chinese
  • 申请详细信息:   CN103342904-A CN10323160 29 Jul 2013
  • 优先权号:   CN10323160

▎ 摘  要

NOVELTY - A water-soluble titanate coupling agent modified graphene is prepared by heating expandable graphite at 1100 degrees C for 15 seconds, oxidizing, dispersing in aqueous solvent to concentration of 0.2-4 mg/mL, stirring, and stripping by mechanical vibration or ultrasonic method; adding 1-500% titanate coupling agent and 10-500 times amount of hydrazine hydrate, and heating to react via water bath, hydrothermal method or microwave-assisted method; and filtering, washing repeatedly, and vacuum drying at 60 degrees C. USE - Method for preparing water-soluble titanate coupling agent modified graphene (claimed) for composites and coatings. ADVANTAGE - The graphene is environment-friendly, stable in water, and long-lived.