• 专利标题:   Preparing graphene by mixing graphite, dispersant and water, grinding and dispersing graphite slurry in colloid mill, homogenizing cooled graphite slurry, continuously circulating graphene slurry, suction filtering and drying.
  • 专利号:   CN107827102-A
  • 发明人:   LI H, WANG B, BAI J, CAI L, HUYANHANXUAN, YU Y, LIAN Y, LIN X, FENG B, ZHANG R, LIU K, FENG Y
  • 专利权人:   INNER MONGOLIA CARBONE GRAPHITE NEW MATERIAL CO LTD
  • 国际专利分类:   C01B032/19
  • 专利详细信息:   CN107827102-A 23 Mar 2018 C01B-032/19 201827 Pages: 10 Chinese
  • 申请详细信息:   CN107827102-A CN11202591 27 Nov 2017
  • 优先权号:   CN11202591

▎ 摘  要

NOVELTY - The method for preparing graphene involves (a) mixing graphite, dispersant and water, (b) grinding and dispersing the graphite slurry in a colloid mill and cooling, (c) transferring the cooled graphite slurry to a high-pressure homogenizer through a diaphragm pump and homogenizing to enable the graphite to be stripped to form uniformly distributed graphene layer, (d) continuously circulating graphene slurry in the high-pressure homogenizer, and (e) suction filtering the graphene slurry, washing with deionized water and drying in a freeze-drying machine to obtain graphene powder. USE - Method is useful for preparing graphene (claimed). ADVANTAGE - The method enables simple and economical preparation of graphene, in an environmentally-friendly manner, and is suitable for industrial mass production. DETAILED DESCRIPTION - The method for preparing graphene involves (a) mixing graphite, dispersant and water in a mass ratio of 3-150:100-5000:0-10 to obtain a graphite slurry, (b) grinding and dispersing the graphite slurry in a colloid mill and transferring the graphite slurry into a material barrel to cool the graphite slurry, (c) transferring the cooled graphite slurry to a high-pressure homogenizer through a diaphragm pump and homogenizing to enable the graphite to be stripped to form uniformly distributed graphene layer, (d) continuously circulating graphene slurry in the high-pressure homogenizer, and (e) suction filtering the graphene slurry, washing with deionized water and drying in a freeze-drying machine to obtain graphene powder with a thickness of less than 10 layers.