• 专利标题:   Preparation of flame retardant used for preparing e.g. polymer material, involves stirring phosphorus-containing flame retardant and graphene oxide grafted with ZIF-8 prepared using 2-methylimidazole, zinc nitrate hexahydrate and copper-loaded graphene oxide, filtering, washing, and drying.
  • 专利号:   CN115466432-A
  • 发明人:   GUAN M, YAN J, SHI W, LU J
  • 专利权人:   COMARKET NEW MATERIALS CO LTD
  • 国际专利分类:   C08K003/30, C08K003/32, C08K005/529, C08K005/5399, C08K009/04, C08K009/12, C08L023/06
  • 专利详细信息:   CN115466432-A 13 Dec 2022 C08K-003/30 202315 Chinese
  • 申请详细信息:   CN115466432-A CN11110360 13 Sep 2022
  • 优先权号:   CN11110360

▎ 摘  要

NOVELTY - Preparation of flame retardant involves: (1) evenly stirring 2-methylimidazole and methanol solution to obtain 2-methylimidazole solution, evenly stirring zinc nitrate hexahydrate and methanol solution to obtain zinc nitrate hexahydrate solution, adding copper-loaded graphene oxide to zinc nitrate hexahydrate solution, ultrasonically dispersing for 4-6 hours, adding 2-methylimidazole solution, ultrasonically dispersing for 10-12 hours, washing with deionized water, adding deionized water, ultrasonically dispersing, adding sodium lignosulfonate aqueous solution, stirring for 60-90 minutes, and drying at 60-70°C to obtain graphene oxide grafted with ZIF-8; and (2) stirring graphene oxide grafted with ZIF-8, phosphorus-containing flame retardant and deionized water at 40-50°C for 2-4 hours, filtering, washing, and drying. USE - Preparation of flame retardant (claimed) used for preparing polymer material, paper and fiber. ADVANTAGE - The method provides flame retardant, which does not adversely affect the mechanical property of the polymer material, and improves the compatibility of graphene oxide grafted with ZIF-8 in polymer material.