• 专利标题:   Aqueous composite high-temperature ink useful for surface decoration, insulation and covering of substrates with small thermal expansion coefficient, preferably high temperature glass coating, comprises glass powder, ceramic powder, ceramic pigment, aqueous varnish, and heat-conducting additive.
  • 专利号:   CN116063879-A
  • 发明人:   WANG S, LIU W, LIU Q, QIN Y, SUN G, LV Y
  • 专利权人:   UNIV SHANTOU
  • 国际专利分类:   C09D011/03
  • 专利详细信息:   CN116063879-A 05 May 2023 C09D-011/03 202347 Chinese
  • 申请详细信息:   CN116063879-A CN10238468 14 Mar 2023
  • 优先权号:   CN10238468

▎ 摘  要

NOVELTY - Aqueous composite high-temperature ink, comprises 30-50 pts. wt. glass powder, 10-23 pts. wt. ceramic powder, 13-25 pts. wt. ceramic pigment, and 15-25 pts. wt. aqueous varnish. USE - The aqueous composite high-temperature ink is useful for surface decoration, insulation and covering of substrates with small thermal expansion coefficient, preferably high temperature glass coating. ADVANTAGE - The aqueous composite high-temperature ink: has resistant to thermal shock, excellent thermal stability, and strong adhesion; is environmentally-friendly; and has simple preparation process. DETAILED DESCRIPTION - INDEPENDENT CLAIMS are included for: preparing aqueous composite high-temperature ink comprising (i) placing stirring tank in a warm water bath at 50-70 ℃ for 15-30 minutes, then adding aqueous varnish into the stirring tank, adding ceramic pigment under low-speed stirring, and stirring at a speed of 150-300 revolutions per minute for 3-5minutes, (ii) adding sequentially ceramic powder, heat-conducting additive and glass powder into the mixture obtained in step (i), stirring at a speed of 500-600 revolutions per minute for 3-5 minutes, mixing uniformly, increasing the stirring speed to 700 revolutions per minute, and stirring for 20-30 minutes, (iii) placing stirring tank in a ball mill for grinding for 2-4 hours, cooling to room temperature; (iv) pouring the semi-finished product composite ink in the stirring tank into a double-roller machine, and repeatedly rolling for more than 3 times to obtain final product; and preparing aqueous composite high-temperature ink-based coating comprising (a) adding 5-8 wt.% aqueous diluent into the aqueous composite high-temperature ink, diluting and stirring uniformly, (b) cleaning the low-expansion glass substrate, wiping the aqueous composite high-temperature ink diluted in the step (a) on a glass substrate panel and drying, and (c) transferring into a sintering furnace and gradually raising the temperature to a heating rate lower than 5 ℃/minute, sintering at 750-850 ℃ for 10-15 minutes, and cooling with the furnace.