• 专利标题:   Producing cross-linked graphene-based film, comprises providing graphene oxide, cross-linking multiple graphene oxides by dispersing in solvent, forming cross-linked graphene oxide film, and reducing the film to obtain cross-linked graphene.
  • 专利号:   KR1667205-B1
  • 发明人:   RAE P C, JUNG H
  • 专利权人:   UNIV SEOUL NAT R DB FOUND
  • 国际专利分类:   C08J005/18, C08K003/04, C08K003/20, C08L101/00
  • 专利详细信息:   KR1667205-B1 18 Oct 2016 C08K-003/20 201676 Pages: 16
  • 申请详细信息:   KR1667205-B1 KR074637 28 May 2015
  • 优先权号:   KR054210

▎ 摘  要

NOVELTY - Producing cross-linked graphene-based film, comprises (a) providing graphene oxide, (b) cross-linking multiple graphene oxides, (c) forming cross-linked graphene oxide film, and (d) reducing the film to obtain cross-linked graphene. The step (b) is carried out. The solvent includes substance containing divalent hydroxy group, -NHR (R is hydrogen or hydrocarbon group), -NCO group and -Cl group or their derivatives. The divalent hydroxy group comprises diol or polyol containing aromatic hydrocarbons and their derivatives. USE - The method is useful for producing cross-linked graphene-based film (claimed). ADVANTAGE - The cross-linked graphene-based film has improved moisture barrier property. DETAILED DESCRIPTION - Producing cross-linked graphene-based film, comprises (a) providing graphene oxide, (b) cross-linking multiple graphene oxides by dispersing in solvent, (c) forming cross-linked graphene oxide film, and (d) reducing the film to obtain cross-linked graphene. The solvent includes substance containing divalent hydroxy group, -NHR (R is hydrogen or hydrocarbon group), -NCO group and -Cl group or their derivatives. The divalent hydroxy group comprises diol or polyol containing aromatic hydrocarbons and their derivatives. The diol containing aromatic hydrocarbons having molecular formula of (CnH2n+2O2) includes ethylene glycol, propanediol, butanediol, pentanediol, hexanediol, heptanediol and octanediol. The polyol containing aromatic hydrocarbons includes glycerol, L-arabitol, xylitol, pentaerythritol, mannitol, sorbitol, dulcitol and sucrose or derivative of hydroquinone, resorcinol, catechol, dihydroxynaphthalene, bisphenol A and myo-inositol.