• 专利标题:   Three-dimensional printing ink material for preparing micro-supercapacitor, is prepared by adding graphene oxide suspension to manganese-ethanolamine composite followed by forming unstable manganese hydroxide and processing.
  • 专利号:   CN110415984-A
  • 发明人:   XU X, ZHENG L, ZHANG Y, WANG W, MA S
  • 专利权人:   UNIV TIANJIN
  • 国际专利分类:   H01G011/24, H01G011/30, H01G011/46, H01G011/86
  • 专利详细信息:   CN110415984-A 05 Nov 2019 H01G-011/24 201989 Pages: 12 Chinese
  • 申请详细信息:   CN110415984-A CN10388362 26 Apr 2018
  • 优先权号:   CN10388362

▎ 摘  要

NOVELTY - A three-dimensional printing ink material is prepared by adding graphene oxide suspension to manganese-ethanolamine composite, stirring, passing oxygen, hydrolyzing to form unstable manganese hydroxide, stirring and dispersing in presence of oxygen to realize co-intercalation of trimanganese tetraoxide into graphene oxide nanosheets and dispersing in solution phase, where the manganese-ethanolamine composite is prepared by uniformly mixing manganese sulfate and ethanolamine in a mass ratio of 3:(10-40) and processing into reddish brown composite, graphene oxide suspension is an aqueous solution, in which graphene oxide is uniformly dispersed, concentration of the graphene oxide is 0.5-2 g/ml, volume ratio of the graphene oxide suspension and manganese-ethanolamine composite is (10-12):3 and the method involves adding graphene oxide suspension to manganese-ethanolamine composite, performing mechanical agitation, stirring at 500-1000 revolutions per minute and reacting for 20-48 hours. USE - Three-dimensional printing ink material for preparing micro-supercapacitor (claimed). ADVANTAGE - The three-dimensional printing ink material comprises trimanganese tetraoxide-graphene oxide composite with excellent electrochemical properties and better conductivity. The micro-supercapacitor has excellent performance. DETAILED DESCRIPTION - INDEPENDENT CLAIMS are also included for the following: (1) a method for preparing three-dimensional printing ink material (2) a use of three-dimensional printing ink material for preparing micro-supercapacitor.