• 专利标题:   Preparation of three-dimensional porous graphene aerogel wave-absorbing material by mixing graphene oxide aqueous solution, reducing agent and anti-freeze agent, dispersing, pre-reducing, freezing, thawing, reducing, aging and freeze-drying.
  • 专利号:   CN113148996-A, CN113148996-B
  • 发明人:   HUANG X, YU G, SHAO G
  • 专利权人:   UNIV NANJING INFORMATION SCI TECHNOLOG
  • 国际专利分类:   B01J013/00, C01B032/19, C01B032/194, C01B032/198
  • 专利详细信息:   CN113148996-A 23 Jul 2021 C01B-032/19 202176 Pages: 9 Chinese
  • 申请详细信息:   CN113148996-A CN10459667 27 Apr 2021
  • 优先权号:   CN10459667

▎ 摘  要

NOVELTY - A three-dimensional porous graphene aerogel wave-absorbing material is prepared by respectively taking graphene oxide aqueous solution, reducing agent and anti-freeze agent, stirring by magnetic force, ultrasonically dispersing to obtain mixed solution, transferring mixed solution into glass bottle, sealing and placing in oven to pre-reduce to obtain pre-reduced graphene hydrogel, freezing at - 30 to - 70 degrees C for 10-60 minutes, thawing at room temperature for 30-60 minutes to obtain freeze thawed pre-reduced graphene hydrogel, sealing and placing in oven for continuously reducing to obtain graphene hydrogel, putting into ethanol/water mixed solution for aging for 24-72 hours and freeze-drying. USE - The method is used for preparing three-dimensional porous graphene aerogel wave-absorbing material. ADVANTAGE - The material has pore size and volume that can be freely and controllable, and realizes free design of different electromagnetic wave absorption by controlling pore size and volume.