• 专利标题:   Preparation of fluorinated graphene involves adding solid graphene oxide into water, ultrasonically processing, adding resultant dispersion into hydrothermal reactor, adding fluorinating agent, reacting, filtering, water washing, and drying.
  • 专利号:   CN107043103-A
  • 发明人:   LIN F, YU C, ZHANG Y
  • 专利权人:   FUJIAN KAIYU MICROCRYSTAL INK CO LTD
  • 国际专利分类:   C01B032/184, C01B032/194
  • 专利详细信息:   CN107043103-A 15 Aug 2017 C01B-032/184 201765 Pages: 4 Chinese
  • 申请详细信息:   CN107043103-A CN10295778 28 Apr 2017
  • 优先权号:   CN10295778

▎ 摘  要

NOVELTY - Preparation of fluorinated graphene involves adding 1-5 pts. wt. solid graphene oxide into 10-50 pts. wt. pure water, ultrasonically processing for 20-50 minutes, obtaining uniform graphene oxide dispersion, adding the resultant dispersion into a hydrothermal reactor lined with a polytetrafluoroethylene, adding 30-65 pts. wt. fluorinating agent, sealing the reactor, placing the reactor in an oven, reacting at 120-200 degrees C for 18-30 hours, naturally cooling the resultant product to room temperature, filtering, washing the resultant filter cake with pure water, and drying. USE - Preparation of fluorinated graphene (claimed). ADVANTAGE - The method enables efficient and safe preparation of fluorinated graphene by simple process with reduced energy consumption. DETAILED DESCRIPTION - Preparation of fluorinated graphene involves adding 1-5 pts. wt. solid graphene oxide into 10-50 pts. wt. pure water, ultrasonically processing for 20-50 minutes, obtaining uniform graphene oxide dispersion, adding the resultant dispersion into a hydrothermal reactor lined with a polytetrafluoroethylene, adding 30-65 pts. wt. fluorinating agent, sealing the reactor, placing the reactor in an oven, reacting at 120-200 degrees C for 18-30 hours, naturally cooling the resultant product to room temperature, filtering, washing the resultant filter cake several times with pure water until pH value becomes neutral, and drying.