• 专利标题:   Lubricating material useful for automobile industry, aviation and aerospace field, comprises nano-manganese oxide particles dispersed on surface of graphene nano-sheet layer.
  • 专利号:   CN113512449-A
  • 发明人:   LUO J, CHEN G, JIN B, HE Y
  • 专利权人:   UNIV TSINGHUA
  • 国际专利分类:   C10N030/06, C10M125/00
  • 专利详细信息:   CN113512449-A 19 Oct 2021 C10M-125/00 202201 Chinese
  • 申请详细信息:   CN113512449-A CN10779791 09 Jul 2021
  • 优先权号:   CN10779791

▎ 摘  要

NOVELTY - Lubricating material comprises graphene nano-sheet layer and nano-manganese oxide particles dispersed on surface of graphene nano-sheet layer. A thickness of the graphene nano-sheet layer is 5-10 nm. An average particle diameter of the nano-manganese oxide particles is 50 to 100 nm. USE - The lubricating material is useful for automobile industry, aviation and aerospace field. ADVANTAGE - The method has simple operation route, and high and stable yield. The lubricating material has good lubricating and anti-friction effect. DETAILED DESCRIPTION - An INDEPENDENT CLAIM is also included for preparing the lubricating material, comprising: (i) mixing potassium permanganate and graphite powder into sulfuric acid solution, heating to generate oxidation reaction to obtain graphene oxide-containing mixed solution; (ii) adding de-ionized water into graphene oxide-containing mixed solution, adding hydrogen peroxide solution, and stirring mixed solution; (iii) adding alkali solution into stirred mixed solution, filtering, washing, and drying to obtain graphene oxide sheet layer with manganese hydroxide particles loaded on surface; (iv) dissolving graphene oxide sheet layer and solid alkali in alcohol solution to obtain suspension; (v) evaporating suspension to obtain alkali-activated graphene oxide sheet layer; and (vi) performing high-temperature reduction treatment to alkali-activated graphene oxide sheet layer under protection of inert gas or vacuum condition, washing, filtering, and drying.