• 专利标题:   Preparing graphene-carbon nanotube heterojunction comprises e.g. processing growth substrate, mechanically stripping graphene on substrate, loading catalyst on growth substrate with graphene, growing single-wall carbon nano tube and cooling.
  • 专利号:   CN113328038-A, CN113328038-B
  • 发明人:   HU Y, ZHANG H, QIAN J, HUANG S
  • 专利权人:   UNIV WENZHOU
  • 国际专利分类:   C01B032/162, C01B032/19, H01L051/05, H01L051/30, H01L051/40
  • 专利详细信息:   CN113328038-A 31 Aug 2021 H01L-051/05 202178 Pages: 10 Chinese
  • 申请详细信息:   CN113328038-A CN10430097 21 Apr 2021
  • 优先权号:   CN10430097

▎ 摘  要

NOVELTY - Preparing graphene-carbon nanotube heterojunction comprises (i) cleaning the growth substrate ultrasonically in ultra-pure water, acetone, ethanol and ultra-pure water, blow drying with high-purity nitrogen, adding the cleaned substrate into a muffle furnace, carrying out high temperature annealing in the air for 2 hours to 900 degrees C, maintaining at 900 degrees C for 8 hours, cooling to 300 degrees C for 10 hours and cooling naturally; (ii) mechanically stripping graphene on the processed growth substrate; (iii) loading catalyst on the growth substrate with graphene and introducing hydrogen and carbon source into the chemical vapor deposition system for growth of single-wall carbon nano tube; and (iv) cooling the system. USE - The method is useful for preparing graphene-carbon nanotube heterojunction. ADVANTAGE - The preparation method: is simple; produces good quality finished product with high electrical properties.; and can weld top growth of the catalyst particles, the carbon nanotubes and graphene together at a high temperature.