• 专利标题:   Preparing graphene/titanium dioxide nanoparticle involves adding titanium glycolate to graphene oxide, ultrasonically processing mixture, and carrying out UV irradiation, freeze-drying process and heat treatment.
  • 专利号:   CN107673444-A
  • 发明人:   YANG D, YU R, YU Z, SHI Y
  • 专利权人:   UNIV BEIJING CHEM TECHNOLOGY
  • 国际专利分类:   C02F001/46, C02F001/461, C02F001/469, C02F103/08
  • 专利详细信息:   CN107673444-A 09 Feb 2018 C02F-001/46 201820 Pages: 10 Chinese
  • 申请详细信息:   CN107673444-A CN10710696 18 Aug 2017
  • 优先权号:   CN10710696

▎ 摘  要

NOVELTY - Method for preparing graphene/titanium dioxide nanoparticle involves (a) adding titanium glycolate to graphene oxide, and ultrasonically processing obtained mixture for 30 minutes to obtain graphene oxide/titanium glycolate dispersion, (b) subjecting the graphene oxide/titanium glycolate dispersion to UV irradiation at 50-600 W for 0.1-30 hours, washing irradiated dispersion using deionized water, and freeze-drying the dispersion, and (c) subjecting freeze-dried dispersion to heat treatment at 250-800 degrees C for 0.1-6 hours under vacuum condition to obtain product. USE - The method is useful for preparing graphene/titanium dioxide nanoparticle (claimed). ADVANTAGE - The method prepares graphene/titanium dioxide nanoparticle having improved stability, low toxicity, large specific surface area, high specific capacitance and good sodium chloride adsorption performance. DETAILED DESCRIPTION - Method for preparing graphene/titanium dioxide nanoparticle involves (a) adding 5-600 mg titanium glycolate to 30 ml graphene oxide (having concentration of 2 mg/ml), and ultrasonically processing obtained mixture for 30 minutes to obtain graphene oxide/titanium glycolate dispersion, (b) subjecting the graphene oxide/titanium glycolate dispersion to UV irradiation at 50-600 W for 0.1-30 hours, washing irradiated dispersion using deionized water, and freeze-drying the dispersion, and (c) subjecting freeze-dried dispersion to heat treatment at 250-800 degrees C for 0.1-6 hours under vacuum condition to obtain product. The particle size of the titanium dioxide is 3-20 nm and the concentration of the titanium dioxide is 10-90 wt.%.