• 专利标题:   Preparing fuel cell cathode catalyst material involves taking iron salt and cobalt salt in beaker, placing graphene oxide in beaker, taking thiourea, heating, naturally cooling, adding powder sample and adding ethylene glycol, and drying.
  • 专利号:   CN113764684-A
  • 发明人:   ZHANG F, GE M, LI M, CUI D
  • 专利权人:   SHANGHAI NAT ENG RES CENT NANOTECHNOLOGY
  • 国际专利分类:   B82Y040/00, B82Y030/00, H01M004/90, H01M004/88
  • 专利详细信息:   CN113764684-A 07 Dec 2021 H01M-004/88 202206 Chinese
  • 申请详细信息:   CN113764684-A CN10944477 17 Aug 2021
  • 优先权号:   CN10944477

▎ 摘  要

NOVELTY - Preparing fuel cell cathode catalyst material comprises (i) taking iron salt and cobalt salt in a beaker, and placing graphene oxide in the beaker; (ii) taking 2 g thiourea in a semi-closed ceramic boat, placing the ceramic boat in a tubular furnace, heating under nitrogen atmosphere and keeping warm for 4 hours, naturally cooling and taking a powder sample; (iii) adding the powder sample into the beakers, and adding 20 ml ethylene glycol, mixing and stirring obtained solution in a water bath, and drying at 80 for 5 hours; (iv) transferring the reactant to 50 ml a high pressure reaction kettle, placing into a blast drying box to react at 160 for 3 hours, and cooling to room temperature; and (v) centrifugally cleaning the obtained product by de-ionized water, and drying to obtain final sample catalyst. USE - The method is useful for preparing fuel cell cathode catalyst material in sensors and supercapacitors. ADVANTAGE - The method is simple, has low reaction temperature, and no subsequent processing conditions. The material has excellent catalytic activity and stability for oxygen reduction reaction.