• 专利标题:   Preparation of high-conductivity graphene involves heating expandable graphite material, dispersing expanded graphite in liquid organic solvent, centrifuging precipitate and drying precipitate.
  • 专利号:   CN104944421-A
  • 发明人:   CAO Y, JIN R, MA J, SUN Y, ZHENG L, ZHANG W
  • 专利权人:   UNIV NORTH CHINA
  • 国际专利分类:   C01B031/04
  • 专利详细信息:   CN104944421-A 30 Sep 2015 C01B-031/04 201608 Pages: 8 Chinese
  • 申请详细信息:   CN104944421-A CN10400084 10 Jul 2015
  • 优先权号:   CN10400084

▎ 摘  要

NOVELTY - Expandable graphite material is heated in heating furnace, to obtain expanded graphite. Expanded graphite is dispersed in liquid organic solvent with surface tension of less than 30 dyn/cm, and ultrasonically processed at -5 degrees C to 100 degrees C for 1.5-3.5 hours, to form precipitate (p1). Precipitate (p1) is removed by centrifugation at 500-1000 rpm and further centrifuged at 1000 rpm, to obtain precipitate (p2). The precipitate (P2) is dried, to obtain graphene with high conductivity. The mass ratio of expanded graphite and organic solvent is 1:100-300. USE - Preparation of high-conductivity graphene (claimed). ADVANTAGE - The method enables preparation of graphene with excellent stability, reduced defects, and high conductivity and yield by economical and simple method, without oxidation-reduction reaction and introduction of impurities.