• 专利标题:   Preparing polymerized nickel nanoparticle decorated on graphene composite by ultrasonicating mixture of graphene oxide and water, adding mixture of nickel nitrate and polyvinyl alcohol, adding hydrazine hydrate, heating to obtain semi-solid solution, heating, dissolving, filtering and drying.
  • 专利号:   IN202111050321-A
  • 发明人:   SHUKLA S K, DAS T R, PATRA S
  • 专利权人:   SHOBHIT ENG TECHNOLOGY INST
  • 国际专利分类:   B01J037/00, B82Y040/00, D01F002/00, C08K003/08, H01M004/36
  • 专利详细信息:   IN202111050321-A 12 Nov 2021 B01J-037/00 202203 Pages: 25 English
  • 申请详细信息:   IN202111050321-A IN11050321 02 Nov 2021
  • 优先权号:   IN11050321

▎ 摘  要

NOVELTY - Method for preparing polymerized nickel nanoparticle decorated on graphene composite involves (i) ultrasonicating mixture of graphene oxide and water to obtain a solution, (ii) adding mixture of nickel nitrate and polyvinyl alcohol to the solution and adding hydrazine hydrate to obtain a homogeneous solution, (iii) heating the homogeneous solution at 60-80 degrees C for 1-3 hours to obtain a semi-solid solution, (iv) placing the semi-solid solution in an autoclave and heating in order to obtain a solid mass, (v) dissolving the solid mass in a mixture of a solvent, filtering and drying to obtain a composite. USE - The method is useful for preparing polymerized nickel nanoparticle decorated on graphene composite. ADVANTAGE - The method enhances the activity of oxygen evolution reaction of the composite, develops polyvinyl alcohol anchored nickel nanoparticle-graphene composite by simple one pot hydrothermal method, develops an efficient oxygen evolution reaction catalyst which delivers a current density of 10 mA cm-2 at very small overpotential and develops a cost effective oxygen evolution reaction catalyst with excellent mechanical and tensile strength.