• 专利标题:   Preparing graphene/hydroxyapatite complex material, by adding phosphate solution into mixed solution, adding calcium and phosphorus, mixing, and carrying out atomization and pyrolysis on mixed solution.
  • 专利号:   CN104961116-A, CN104961116-B
  • 发明人:   LIN J
  • 专利权人:   FUJIAN NORCY SCI PARK DEV CO LTD, FUJIAN NORCY SCI PARK DEV CO LTD
  • 国际专利分类:   C01B025/32, C01B031/04, C01B032/182
  • 专利详细信息:   CN104961116-A 07 Oct 2015 C01B-025/32 201611 Pages: 6 Chinese
  • 申请详细信息:   CN104961116-A CN10379499 02 Jul 2015
  • 优先权号:   CN10379499

▎ 摘  要

NOVELTY - Method for preparing graphene/hydroxyapatite complex material, involves (a) preparing mixed solution (I) comprising 0.5-10 %mass graphene and 0.5-3 %mass calcium ions, (b) adding phosphate solution into the mixed solution (I) in a mass ratio of 0.5-3:1, adding calcium and phosphorus to the mixture, and mixing materials to obtain mixed solution (II), and (c) carrying out atomization and pyrolysis on the mixed solution (II) by adopting ultrasonic pyrolysis. USE - The method is useful for preparing graphene/hydroxyapatite complex material (claimed). ADVANTAGE - The prepared material has good mechanical property, absorbance effect, and biocompatibility. DETAILED DESCRIPTION - Method for preparing graphene/hydroxyapatite complex material, involves (a) preparing mixed solution (I) comprising 0.5-10 %mass graphene and 0.5-3 %mass calcium ions, (b) adding phosphate solution into the mixed solution (I) in a mass ratio of 0.5-3:1, adding calcium and phosphorus to the mixture, and mixing materials to obtain mixed solution (II), and (c) carrying out atomization and pyrolysis on the mixed solution (II) by adopting ultrasonic pyrolysis, where ultrasonic power is 1000-1200 W, the transducer frequency is 5-7 MHz, the pyrolysis temperature is 550-650 degrees C and the pyrolysis reaction time is 10 minutes.