• 专利标题:   Preparing graphene coated white carbon black nano composite material comprises e.g. adding graphite oxide and cyclomethicone into deionized water, stirring, adding polysulfide-polyethylene glycol resin, sonicating, drying and grinding.
  • 专利号:   CN108530952-A
  • 发明人:   PENG G
  • 专利权人:   UNIV NINGBO TECHNOLOGY
  • 国际专利分类:   C08K003/36, C08K009/10, C09C001/30, C09C003/06, C09C003/10, C09C003/12
  • 专利详细信息:   CN108530952-A 14 Sep 2018 C09C-001/30 201871 Pages: 8 Chinese
  • 申请详细信息:   CN108530952-A CN10314760 10 Apr 2018
  • 优先权号:   CN10314760

▎ 摘  要

NOVELTY - Preparing graphene coated white carbon black nano composite material comprises (i) adding 0.1-0.5 g graphite oxide and 1-3 g cyclomethicone into 100 ml deionized water and stirring at room temperature for 20 minutes at 200 revolutions/minute; (ii) adding 1 g polysulfide(PS)-polyethylene glycol (PEG) resin into the above solution, heating to 60-80 degrees C, and stirring at 300 revolutions/minute for 3 hours; (iii) cooling above solution to room temperature, introducing into photoreactor, irradiating and reacting by an YLS-2000 laser for 6 hours to obtain a black gel; (iv) placing gel in 150 ml volume mixture of deionized water and n-butanol at ratio 1:1, sonicating at 80-120 W at 30-50 KHz for 2-3 hours, filtering under suction filter and washing filter cake using deionized water until the quality is unchanged; and (v) drying filter cake under vacuum at 50-80 degrees C for 8-10 hours, and grinding dried filter cake. USE - The method is useful for preparing graphene coated white carbon black nano composite material. ADVANTAGE - The method is economical, simple and rapid, and does not require any photo catalyst or reducing agent and produces environmentally-friendly and stable material.