• 专利标题:   Graphene material preparation by stirring graphite suspension in container installed with gear set at low speed, then high speed centrifuging to obtain upper layer solution as single layer graphene solution, and concentrating solution.
  • 专利号:   CN102583350-A, CN102583350-B
  • 发明人:   GUO G, KONG M, QIN X, SONG C, WANG N, XIN H, ZHANG J, ZHU X
  • 专利权人:   CHINESE ACAD SCI HEFEI INST PHYSICAL SCI, CHINESE ACAD SCI HEFEI INST PHYS SCI
  • 国际专利分类:   C01B031/04
  • 专利详细信息:   CN102583350-A 18 Jul 2012 C01B-031/04 201308 Pages: 5 Chinese
  • 申请详细信息:   CN102583350-A CN10046788 28 Feb 2012
  • 优先权号:   CN10046788

▎ 摘  要

NOVELTY - Graphene material is prepared by dissolving graphite powder in organic solvent or water to form suspension, putting suspension into a container installed with gear set and stirring suspension at low speed of 1-800 revolutions/minute (rpm) for 5-30 hours; ultrasonically treating obtained slurry for 5-2 hours, and then high speed centrifuging at 1000-4000 rpm for 5 minutes to obtain upper layer solution as single layer graphene solution; and concentrating upper layer solution and separating to obtain graphene powder or graphene solution. USE - Method for preparing graphene material (claimed). ADVANTAGE - The method utilizes continuous gear rotation to stir graphite suspension, thus overcoming defect and low yield when using mechanical method. Further, the method has high efficiency and obtains high quality product. DETAILED DESCRIPTION - Preparation of graphene material comprises: (A) dissolving graphite powder in organic solvent or water to form suspension, then putting suspension into a container installed with gear set and stirring the suspension at low speed of 1-800 revolutions/minute (rpm) for 5-30 hours, and taking out obtained slurry; (B) ultrasonically treating the slurry for 5-2 hours, then high speed centrifuging at 1000-4000 rpm for 5 minutes, ensuring not to peel off graphite particles precipitate on bottom layer, and obtaining upper layer solution as single layer graphene solution; and (C) concentrating and separating upper layer solution to obtain graphene powder or graphene solution.