• 专利标题:   Yttrium aluminum garnet nano fiber enhanced graphene oxide sealing resin includes yttrium aluminum garnet nano fiber, titanium acid ester coupling agent, melamine, aqueous formaldehyde, graphene oxide and trifluoroethyl methacrylate.
  • 专利号:   CN104804155-A
  • 发明人:   ZHANG Q
  • 专利权人:   WUHU VALUABLE SKILL AMUSEMENT EQUIP CO
  • 国际专利分类:   C08G012/32, C08K013/06, C08K003/04, C08K007/08
  • 专利详细信息:   CN104804155-A 29 Jul 2015 C08G-012/32 201577 Pages: 4 Chinese
  • 申请详细信息:   CN104804155-A CN10220460 04 May 2015
  • 优先权号:   CN10220460

▎ 摘  要

NOVELTY - Yttrium aluminum garnet nano fiber enhanced graphene oxide sealing resin comprises 0.3-0.5 pt. wt. yttrium aluminum garnet nano fiber, 0.03-0.05 pt. wt. titanium acid ester coupling agent, 20-25 pts. wt. melamine, 40-45 pts. wt. aqueous formaldehyde, 1.8-2.1 pts. wt. graphene oxide, 0.7-0.9 pt. wt. trifluoroethyl methacrylate, 0.7-0.9 pt. wt. polyacrylonitrile, dimethylformamide, 0.2-0.3 pt. wt. polyoxyethylene, dimethylformamide/dichloromethane mixture at mass ratio of 1:1, 0.3-0.5 pt. wt. t-butyl hydroperoxide, citric acid, pH regulator and ethanol. USE - Yttrium aluminum garnet nano fiber enhanced graphene oxide sealing resin. ADVANTAGE - The yttrium aluminum garnet nano fiber enhanced graphene oxide sealing resin has high transparency, high stability and high temperature resistance property. DETAILED DESCRIPTION - An INDEPENDENT CLAIM is included for the preparation of yttrium aluminum garnet nano fiber enhanced graphene oxide sealing resin comprising dissolving polyacrylonitrile in dimethyl formamide, polyethylene oxide in dimethyl formamide/dichloromethane mixture, mixing two solutions, adding yttrium aluminum garnet nano fiber, titanium acid ester coupling agent and graphene oxide, stirring, adding trifluoroethyl methacrylate and t-butyl hydroperoxide, heating at 60-70 degrees C, stirring for 1-2 hours, filtering, washing residue with ethanol 2-3 times to obtain modified graphene oxide, mixing melamine in 37% formaldehyde, heating at 70-75 degrees C, stirring to dissolve, adding modified graphene oxide, stirring for 10-20 minutes, adding pH regulator, adjusting pH to 8-9, reacting for 3-4 hours to obtain graphene oxide containing melamine resin prepolymer, placing in oven under vacuum, heating at 30 degrees C, adjusting pH to 5-6 using citric acid, and curing for 8-9 hours.