• 专利标题:   Graphene preparation by melting sodium chloride, potassium chloride and zinc chloride, adding graphite fluoride into molten salt and performing thermal intercalation, centrifuging intercalated complex, filtering, and drying filter cake.
  • 专利号:   CN103588195-A
  • 发明人:   LI Y, FENG W, FENG Y, SUN Z
  • 专利权人:   UNIV TIANJIN
  • 国际专利分类:   C01B031/04
  • 专利详细信息:   CN103588195-A 19 Feb 2014 C01B-031/04 201426 Pages: 7 Chinese
  • 申请详细信息:   CN103588195-A CN10539828 01 Nov 2013
  • 优先权号:   CN10539828

▎ 摘  要

NOVELTY - Graphene is prepared by uniformly mixing and melting sodium chloride, potassium chloride and zinc chloride at mass ratio of 1:1:3 to obtain molten salt; adding graphite fluoride into molten salt at mass ratio of 1-5:50, heating to 200-350 degrees C for 6-12 hours, and performing thermal intercalation; naturally cooling obtained intercalated complex to room temperature at 20-25 degrees C, adding organic solvent, ultrasonically centrifuging, and removing lower layer solid; and filtering obtained solution, washing filter cake and drying. USE - Method for preparing graphene (claimed). ADVANTAGE - The method does not need high temperature, high vacuum condition and special reaction instrument. It has simple operation and low preparation cost. The obtained graphene sheet has large surface area and high tactility.