• 专利标题:   Preparing light resistance paint comprises e.g. dissolving sodium dodecyl sulfate in water, adding graphene and nano-material, emulsifying to obtain graphene emulsion, adding acrylic acid and potassium persulfate solution, and reacting.
  • 专利号:   CN103194135-A, CN103194135-B
  • 发明人:   DUAN B, HUANG J, LU X, PAN Y, YE H, ZHAO Z, ZUO G
  • 专利权人:   DUAN B
  • 国际专利分类:   C09D133/14, C09D007/12
  • 专利详细信息:   CN103194135-A 10 Jul 2013 C09D-133/14 201422 Pages: 5 Chinese
  • 申请详细信息:   CN103194135-A CN10158409 02 May 2013
  • 优先权号:   CN10158409

▎ 摘  要

NOVELTY - Preparing light resistance paint comprises (i) dissolving sodium dodecyl sulfate in water, adding graphene, flatting agent and nano-material, emulsifying in a shear emulsifier at the speed of 500-1000 revolutions/minute for 60-80 minutes, controlling ultrasonic sound intensity at 0.12-0.3 W/cm2 and emulsifying for 20-50 minutes to obtain graphene emulsion; and (ii) adding acrylic acid, hydroxyethyl acrylate and polycarbonate diol into the graphene emulsion at 70-90 degrees C, dropping potassium persulfate solution at constant speed for 1 hour, and reacting for 2-4 hours. USE - The method is useful in preparing light resistance paint (claimed). ADVANTAGE - The method is simple. The paint has good light resistance performance and strong adhesion force. DETAILED DESCRIPTION - Preparing light resistance paint comprises (i) dissolving sodium dodecyl sulfate in water, adding graphene, flatting agent and nano-material, emulsifying in a shear emulsifier at the speed of 500-1000 revolutions/minute for 60-80 minutes, controlling ultrasonic sound intensity at 0.12-0.3 W/cm2 and emulsifying for 20-50 minutes to obtain graphene emulsion, where the amount of each component as follows: 5-9% sodium dodecyl sulfate, 1-3% graphene, 0.1-0.5% flatting agent, 0.2-0.6% nano-material and water (remaining amount); and (ii) adding acrylic acid, hydroxyethyl acrylate and polycarbonate diol into the graphene emulsion at 70-90 degrees C, dropping potassium persulfate solution at constant speed for 1 hour, and reacting for 2-4 hours, where the amount of each component as follows 1-5% acrylic acid, 25-35% hydroxyethyl acrylate, 2-8% polycarbonate diol, 0.5-0.9% potassium persulfate and 64-74.6% graphene emulsion.