• 专利标题:   Preparation of copper-based olefinic alloy involves cold briquetting graphene and copper and/or copper alloy mixed powder, degassing in quartz tube, sintering, cooling, heat preserving and extruding in preset squeeze ratio.
  • 专利号:   CN105063403-A
  • 发明人:   DAI S, YANG C, HONG Q, YAN S
  • 专利权人:   AVIATION IND CORP CHINA BEIJING GREAT WA
  • 国际专利分类:   C22C001/05, C22C001/10, C22C009/00, C22F001/08
  • 专利详细信息:   CN105063403-A 18 Nov 2015 C22C-001/10 201632 Pages: 8 English
  • 申请详细信息:   CN105063403-A CN10382240 25 Jun 2015
  • 优先权号:   CN10382240

▎ 摘  要

NOVELTY - Graphene and copper and/or copper alloy mixed powder comprising 3-10 wt.% graphene and remainder of copper and/or copper alloy powder, is subjected to cold briquetting process, degassed under vacuum condition for 2-4 hours in quartz tube in the vacuum degree of 1x 10-3 Pa. The quartz tube is heated at 850-950 degrees C for 2-4 hours, cooled, heat preserved at 800-900 degrees C for 24-48 hours, and subjected to hot extrusion process in the squeeze ratio of 15:1-20:1 to obtain copper-based olefinic alloy. USE - Preparation of copper-based olefinic alloy (claimed). ADVANTAGE - The method efficiently and economically provides copper-based olefinic alloy by simple method with high productivity. DETAILED DESCRIPTION - Graphene dispersion solution is obtained by configuring solution, adding graphene into solution, placing in ultrasonic wave oscillator and stirring. Copper and/or copper alloy powder is added to obtained graphene monodisperse solution and milled in ball mill jar for 20-40 hours. The obtained mixed solution is baked at 50-60 degrees C and dried to obtain graphene and copper and/or copper alloy mixed powder comprising 3-10 wt.% graphene and remainder of copper and/or copper alloy powder. The resultant powder is subjected to cold briquetting process, degassed under vacuum condition for 2-4 hours in quartz tube in the vacuum degree of 1x 10-3 Pa. The quartz tube is heated at 850-950 degrees C for 2-4 hours, cooled, heat preserved at 800-900 degrees C for 24-48 hours, and subjected to hot extrusion process in the squeeze ratio of 15:1-20:1 to obtain copper-based olefinic alloy.