• 专利标题:   Preparing porous graphene comprises taking crystalline flake graphite in a crucible, adding concentrated sulfuric acid and concentrated nitric, stirring, oxidizing, micro waving and nitrogen doping.
  • 专利号:   CN106219533-A, CN106219533-B
  • 发明人:   LUO Z, ZHAO Y, LUO K
  • 专利权人:   UNIV GUILIN TECHNOLOGY, UNIV GUILIN TECHNOLOGY
  • 国际专利分类:   C01B031/04, C01B032/184
  • 专利详细信息:   CN106219533-A 14 Dec 2016 C01B-031/04 201710 Pages: 5 Chinese
  • 申请详细信息:   CN106219533-A CN10633798 04 Aug 2016
  • 优先权号:   CN10633798

▎ 摘  要

NOVELTY - Preparing porous graphene comprises (i) taking 1 g crystalline flake graphite in a crucible, adding concentrated sulfuric acid and concentrated nitric in the volume ratio of 3:1, stirring and oxidizing for 2-5 hours at 30-60 degrees C to obtain oxidized graphite, (ii) adding the graphite oxide in the crucible, micro waving for 3-8 seconds at 800-1000 W power in a microwave oven to obtain the porous graphene, (iii) placing in nitride, ammonia or air atmosphere cold plasma generating device, the gas flow rate is 1-5- l/minute at 10-40 W and nitrogen doping for 10-60 minutes. USE - The method is useful for preparing porous graphene (claimed). ADVANTAGE - The method consumes low energy, is easy to operate, environmentally-friendly. The product structure obtained has good stability and high nitrogen doping ability.