▎ 摘 要
NOVELTY - Preparation of molybdenum disulfide-graphene hybrid material involves using electrochemical electrodes comprising a graphite material, an electrolyte solution comprising ammonium tetrathiomolybdate potassium hydroxide and ammonium sulfate and a power source which is direct current power having a voltage of 60-80 V, and cleaning the obtained hybrid material by filtering the electrolyte from the hybrid material using a filtration membrane comprising polyvinylidene fluoride, washing the obtained material with deionized water and washing with pure alcohol and drying. USE - Preparation of molybdenum disulfide-graphene hybrid material. ADVANTAGE - The method enables simple preparation of molybdenum disulfide-graphene hybrid material. The method is carried out at ambient temperature conditions without requiring vacuum environment. The method is suitable for large scale preparation. DETAILED DESCRIPTION - Preparation of molybdenum disulfide-graphene hybrid material by an electrochemical method, involves using electrochemical electrodes comprising a graphite material, an electrolyte solution comprising ammonium tetrathiomolybdate potassium hydroxide and ammonium sulfate and a power source which is direct current power having a voltage of 60-80 V, and cleaning the obtained molybdenum disulfide-graphene hybrid materials by filtering the electrolyte from the molybdenum disulfide-graphene hybrid material using a filtration membrane comprising polyvinylidene fluoride and having a pore size of 0.2 mu m, washing the obtained material with deionized water and washing with pure alcohol and drying the obtained material in an drying oven.