• 专利标题:   Preparing graphene-rare earth hybrid microstructure titanium-based composition material comprises e.g. dispersing graphene in solvent by ultrasonic pre-dispersion assisted mechanical stirring obtaining a graphene dispersion.
  • 专利号:   CN110434347-A
  • 发明人:   DONG L, HUO W, LU J, ZHANG Y, LIU Y, LI L, LI D
  • 专利权人:   XIAN RARE METAL MATERIAL RES INST CO LTD
  • 国际专利分类:   B22F001/02, B22F003/105, B22F009/04, C22C001/05, C22C001/10, C22C014/00
  • 专利详细信息:   CN110434347-A 12 Nov 2019 B22F-009/04 201989 Pages: 9 Chinese
  • 申请详细信息:   CN110434347-A CN10814653 30 Aug 2019
  • 优先权号:   CN10814653

▎ 摘  要

NOVELTY - Preparing graphene-rare earth hybrid microstructure titanium-based composition material comprises (i) dispersing the graphene in solvent by ultrasonic pre-dispersion assisted mechanical stirring, obtaining a graphene dispersion; (ii) performing high-energy ball milling of rare earth-titanium powder, rare earth element-containing substance and titanium or titanium alloy powder by high energy and mixing to obtain rare earth-titanium mixed powder; (iii) adding graphene dispersion obtained in the step (i) to the rare earth-titanium based mixed powder obtained in the step (ii), mechanically shearing to a semi-solid state under conditions of 80-100 degrees C, then carrying out low energy ball milling, mixing, and then vacuum-drying to obtain ternary mixed powder; and (iv) sintering the ternary mixed powder obtained in the step (iii). USE - The method is useful for preparing graphene-rare earth hybrid microstructure titanium-based composition material. ADVANTAGE - The method: adopts two-step mixing method with graphene-ternary rare earth mixed micro-structure mixed powder and sintering to obtain graphene-rare earth mixed micro-structure titanium-based composition material; adopts the composition material in the ball containing rare earth element substance particle, which has dispersion strengthening and strengthening grain boundary; adopts titanium carbide in situ synthesized, which has dispersion effect of strengthening; adopts grapheme, which has the function of transferring load, three cooperative strengthening, which improves graphene-rare earth hybrid strength mechanical properties of microstructure titanium base composition material.