• 专利标题:   Preparing 5,5'-diamino-3,3'-1,2,4-triazole cobalt salt based graphene material comprises e.g. dispersing graphene in deionized water, adding aqueous 5,5'-diamino-3,3'-1,2,4-triazole cobalt salt solution, heating, drying and grinding.
  • 专利号:   CN110980713-A
  • 发明人:   ZHU J, WU D, YANG X, LIN R, FANG J
  • 专利权人:   UNIV GUANGDONG PETROCHEMICAL TECHNOLOGY
  • 国际专利分类:   C01B032/194
  • 专利详细信息:   CN110980713-A 10 Apr 2020 C01B-032/194 202035 Pages: 8 Chinese
  • 申请详细信息:   CN110980713-A CN11360900 26 Dec 2019
  • 优先权号:   CN11360900

▎ 摘  要

NOVELTY - Preparing 5,5'-diamino-3,3'-1,2,4-triazole cobalt salt based graphene material comprises dispersing graphene in deionized water, then adding aqueous 5,5'-diamino-3,3'-1,2,4-triazole cobalt salt solution and heating at 50-100 degrees C for 30-60 minutes, cooling to 0-4 degrees C, and drying to obtain graphene-coated 5,5'-diamino-3,3'-1,2,4-triazole cobalt salt eutectic, grinding it into powder and placing it in a tube furnace at 500-800 degrees C for 3-5 hours to obtain nitrogen-cobalt co-doped graphene material, where the mass ratio between graphene and 5,5'-diamino-3,3'-1,2,4-triazole cobalt salt in aqueous 5,5'-diamino-3,3'-1,2,4-triazole cobalt salt solution is 1:1-10. USE - The method is useful for preparing 5,5'-diamino-3,3'-1,2,4-triazole cobalt salt based graphene material. ADVANTAGE - The method: does not use adhesives and other additives.