• 专利标题:   Method for preparing graphene/nano-silicon lithium ion battery cathode material, involves utilizing liquid phase physical technique, dissolving surfactant in deionized water, stirring, followed by adding graphite powder and silicon powder.
  • 专利号:   CN104993109-A, CN104993109-B
  • 发明人:   LIU H, MA S, SHEN Z, ZHANG X
  • 专利权人:   UNIV BEIJING AERONAUTICS ASTRONAUTICS, UNIV BEIHANG
  • 国际专利分类:   H01M010/0525, H01M004/36, H01M004/38, H01M004/587
  • 专利详细信息:   CN104993109-A 21 Oct 2015 H01M-004/36 201610 Pages: 8 Chinese
  • 申请详细信息:   CN104993109-A CN10294379 02 Jun 2015
  • 优先权号:   CN10294379

▎ 摘  要

NOVELTY - A graphene/nano-silicon lithium ion battery cathode material preparing method utilizing liquid phase physical technique, dissolving surfactant in deionized water, stirring, adding graphite powder and nano-silicon powder, stirring, ultrasonic dispersion and adding dispersion solution to obtain mixed dispersion. The obtained dispersion is involved ultrasonic treatment, placed in centrifuge tube, performed centrifugal separation treatment, followed by taking upper solution, performing vacuum filtration, drying to form grey powder, placing into quartz boat and performing calcination. USE - Method for preparing graphene/nano-silicon lithium ion battery cathode material. ADVANTAGE - The method enables preparing graphene/nano-silicon lithium ion battery cathode material with good dispersibility, avoiding agglomeration of liquid phase method prepared graphene, omitting secondary dispersion of liquid phase physical method prepared graphene and improving lithium ion battery cathode material performance in a simple manner. DETAILED DESCRIPTION - A graphene/nano-silicon lithium ion battery cathode material preparing method utilizing liquid phase physical technique, dissolving surfactant in deionized water, stirring, adding graphite powder and nano-silicon powder, stirring to dissolve, ultrasonic dispersion, adding dispersion solution and stirring to obtain graphite powder and nano-silicon powder mixed dispersion. The obtained dispersion is involved ultrasonic treatment, placed in centrifuge tube, performed centrifugal separation treatment, followed by standing solution, taking upper solution, performing vacuum filtration, drying to form grey powder, placing into quartz boat with argon-filled different tube furnace, controlling gas flow rate and performing calcination to obtain graphene/nano-silicon composite material.