• 专利标题:   Preparation of graphene-containing lithium-based grease involves dissolving 12-hydroxystearic acid in base oil, pouring mixture into fat-forming kettle, heating, adding aqueous solution of lithium hydroxide and stirring.
  • 专利号:   CN108467763-A
  • 发明人:   ZHANG J, WANG A, YIN H
  • 专利权人:   UNIV JIANGSU
  • 国际专利分类:   C10M125/02, C10M169/00, C10M177/00, C10N030/06
  • 专利详细信息:   CN108467763-A 31 Aug 2018 C10M-169/00 201864 Pages: 5 Chinese
  • 申请详细信息:   CN108467763-A CN10064069 23 Jan 2018
  • 优先权号:   CN10064069

▎ 摘  要

NOVELTY - Preparation of graphene-containing lithium-based comprises dissolving 12-hydroxystearic acid in 1/2 m1 base oil, pouring mixture into fat-forming kettle, heating at 90 degrees C for 1-2 hours, heating autoclave at 110-120 degrees C for 20 minutes, adding aqueous solution of lithium hydroxide, saponifying solution by constant temperature reaction for 5-6 hours, heating at 170-180 degrees C for 10 minutes after safonification, removing excess water by stirring at constant temperature for 2-3 hours, adding 1/2 m1 base oil and antioxidant, heating at 200-210 degrees C for 3 hours, keeping at this temperature for 5 minutes, pouring product into stainless steel cup, quenching, cooling, grinding by three-roller machine to obtain lithium-based grease of mass m3, taking base oil of mass m2, adding graphene, stirring with glass, ultrasonically treating for 1-2 hours, mixing lithium-based grease m3 with graphene-containing base oil, dispersing and mixing by grinding wheel for 2-3 hours. USE - Method for preparing graphene-containing lithium-based grease. ADVANTAGE - The product has enhanced friction performance and compression performance.