• 专利标题:   Preparing surface-modified flame retardant involves mixing silane coupling agent with benzene, adding azobisisobutyronitrile, adding graphene oxide to water, ultrasonic treating, and adding dispersion with zinc and tin salts.
  • 专利号:   CN105295100-A, CN105295100-B
  • 发明人:   GAO T, LI Z, ZHANG Z
  • 专利权人:   UNIV HENAN
  • 国际专利分类:   C08K003/04, C08K003/24, C08K009/04, C08K009/06, C08L027/06
  • 专利详细信息:   CN105295100-A 03 Feb 2016 C08K-009/04 201637 Pages: 8 English
  • 申请详细信息:   CN105295100-A CN10625840 28 Sep 2015
  • 优先权号:   CN10625840

▎ 摘  要

NOVELTY - A surface-modified flame retardant is prepared by mixing silane coupling agent with benzene, adding azobisisobutyronitrile, continuing reaction, filtering, and evaporating excess benzene to give colorless liquid; adding graphene oxide to water, ultrasonic treating for 10-120 minutes, and obtaining graphene oxide dispersion; adding the dispersion with zinc and tin salts, reacting at 5-80 degrees C for 2-6 hours, filtering, and washing to obtain nano-zinc tin oxide/graphene filter cake; and adding the filter cake with ethanol, and performing ultrasonic dispersion. USE - Method for preparing surface-modified flame retardant (claimed). DETAILED DESCRIPTION - Preparing surface-modified flame retardant comprises mixing silane coupling agent with benzene, adding azobisisobutyronitrile, continuing reaction, filtering, and evaporating excess benzene to give colorless liquid; adding graphene oxide to water at room temperature to 80 degrees C, ultrasonic treating for 10-120 minutes, and obtaining graphene oxide dispersion; adding the dispersion with zinc and tin salts, reacting at 5-80 degrees C for 2-6 hours, filtering, and washing to obtain nano-zinc tin oxide/graphene filter cake; and adding the filter cake with ethanol, performing ultrasonic dispersion for 10-60 minutes, warming to 50-80 degrees C, adding surface modifier, adjusting pH to 8-9, reacting for 1-6 hours, washing reaction product with water, and drying.