• 专利标题:   Preparation of manganese ferrite nanoparticles-graphene composite used as electromagnetic shielding material, by oxidizing graphite with potassium permanganate, diluting, adding hydrogen peroxide and ferric salt, adjusting pH, and reducing.
  • 专利号:   CN103341346-A, CN103341346-B
  • 发明人:   BAO J, BAO Z, LI X
  • 专利权人:   JIANGSU INST ENVIRONMENTAL SCI, SUZHOU YUHAO NANO MATERIALS CO LTD
  • 国际专利分类:   B01J020/20, B01J020/28, B01J020/30, B01J023/889, H05K009/00
  • 专利详细信息:   CN103341346-A 09 Oct 2013 B01J-020/20 201405 Pages: 8 Chinese
  • 申请详细信息:   CN103341346-A CN10260188 26 Jun 2013
  • 优先权号:   CN10260188

▎ 摘  要

NOVELTY - Preparation of manganese ferrite nanoparticles-graphene composite comprises oxidizing graphite with potassium permanganate to obtain graphene oxide, ultrasonically processing, diluting with water to obtain homogenous manganese-containing graphene oxide solution, adding hydrogen peroxide to reduce permanganate ions into divalent manganese ions, adding ferric and manganous salts, and uniformly stirring; adjusting pH to 8-13 with alkaline aqueous solution; and adding reducing agent and heating to 70-99 degrees C, maintaining temperature and stirring for 0.5-24 hours, magnetically separating, and drying. USE - Method for preparing manganese ferrite nanoparticles-graphene composite used as electromagnetic shielding material (claimed). ADVANTAGE - The method is simple and environmentally friendly, and has low cost. The obtained composite has specific surface area of 5-100 m2/g and electromagnetic shielding efficiency of 15-90 dB at 5 kHz to 18 GHz.