• 专利标题:   Preparation of alpha-ferric oxide quantum point/nitrogen-doped graphene composite material by mixing hydroxyl-containing organic compound and water, ultrasonically treating with alkali source, inorganic iron and graphene oxide, and reacting.
  • 专利号:   CN104607228-A
  • 发明人:   CUI F, GAO S, SHI W, TIAN J, SHAO P
  • 专利权人:   HARBIN INST TECHNOLOGY
  • 国际专利分类:   B01J027/24, C02F001/72
  • 专利详细信息:   CN104607228-A 13 May 2015 B01J-027/24 201563 Pages: 11 Chinese
  • 申请详细信息:   CN104607228-A CN10036230 23 Jan 2015
  • 优先权号:   CN10036230

▎ 摘  要

NOVELTY - Preparation of alpha -ferric oxide quantum point/nitrogen-doped graphene composite material comprises taking hydroxyl-containing organic compound, adding deionized water, stirring and mixing to obtain organic matter solution; taking alkali source and inorganic iron aqueous solution, adding organic matter solution and stirring to form homogeneous transparent liquid; adding graphene oxide, ultrasonically treating and stirring to obtain suspension; and adding into hydrothermal reaction kettle, reacting, naturally cooling, centrifuging, washing with deionized water, washing with ethanol and drying. USE - Method for preparing alpha -ferric oxide quantum point/nitrogen-doped graphene composite material (claimed). ADVANTAGE - The method has mild reaction condition, simple device, low reagent cost, high safety and no toxicity. It is suitable for large-scale production. DETAILED DESCRIPTION - Preparation of alpha -ferric oxide quantum point/nitrogen-doped graphene composite material comprises: (A) taking hydroxyl-containing organic compound, adding deionized water at ratio of 1 g: (0.5-1 mL), stirring and mixing for 5-10 minutes to obtain organic matter solution; (B) taking alkali source and 0.05-0.5 mol/L inorganic iron aqueous solution, adding organic matter solution and stirring for 5-10 minutes to form homogeneous transparent mixed liquid; (C) adding graphene oxide, ultrasonically treating for 0.3-2.0 hours and stirring for 2.0-4.0 hours to obtain stable suspension; and (D) adding into hydrothermal reaction kettle, reacting at 100-200 degrees C for 5-36 hours, naturally cooling to room temperature, centrifuging, washing with deionized water for 3 times, washing with ethanol for 2 times and drying at 50 degrees C for 12 hours.