• 专利标题:   Preparing graphene-modified prismatic carbon nitride by hydrothermally treating melamine, mixing supramolecular precursor with graphite oxide solution, filtering precipitate and washing, and freeze-drying and calcining.
  • 专利号:   CN111330611-A
  • 发明人:   FU Y, YU C, WANG X, ZHU J, HUANG T, PENG Q, SHI L
  • 专利权人:   UNIV NANJING SCI TECHNOLOGY
  • 国际专利分类:   B01J027/24, C01B003/04
  • 专利详细信息:   CN111330611-A 26 Jun 2020 B01J-027/24 202062 Pages: 9 Chinese
  • 申请详细信息:   CN111330611-A CN11555592 19 Dec 2018
  • 优先权号:   CN11555592

▎ 摘  要

NOVELTY - Method for preparing graphene-modified prismatic carbon nitride, involves (a) hydrothermally treating melamine to obtain a supramolecular precursor, (b) mixing the supramolecular precursor with a graphite oxide solution uniformly dispersed by ultrasound, and shaken evenly on a shaker, (c) filtering the precipitate obtained in the step (b) and washing, and freeze-drying the obtained solid, and (d) calcining the solid obtained in the step (c) at 550 plus minus 10 degrees C for 4-6 hours to prepare graphene-modified prismatic carbon nitride. USE - The method is used for preparing graphene-modified prismatic carbon nitride which is used as a catalyst in photocatalytic hydrogen production (all claimed). ADVANTAGE - The method increases the specific surface area, exposes more active sites, improves the absorption and utilization of visible light, benefits the separation and migration of photo-generated carriers, and improves the catalytic activity of visible light hydrogen production.