• 专利标题:   Preparation of functionalized graphene coated probe involves treating metal core front with acid, washing, drying, converting to 3-aminopropyl-triethoxysilane, immersing in graphite oxide, drying, immersing in aqueous ammonia and drying.
  • 专利号:   CN106823461-A
  • 发明人:   SONG A, WEI L, JIA Z, WANG J, DAN E, CENG Z
  • 专利权人:   GANSU POLITICAL SCI LAW INST
  • 国际专利分类:   B01D015/10, B01D015/20, B01J020/22, B01J020/28, B01J020/30, G01N001/34
  • 专利详细信息:   CN106823461-A 13 Jun 2017 B01D-015/10 201747 Pages: 11 Chinese
  • 申请详细信息:   CN106823461-A CN10112073 28 Feb 2017
  • 优先权号:   CN10112073

▎ 摘  要

NOVELTY - Preparation of functionalized graphene coated probe comprises treating metal core front with acid, washing and drying; converting to 3-aminopropyl-triethoxysilane; immersing in 0.1 wt.% graphite oxide and drying; immersing in aqueous ammonia solution, reacting at 60-80 degrees C, washing, drying, reacting with acetyl chloride, washing and drying; repeating (3)-(4) steps 4-7 times until coating thickness is 50-100 mu m; passing through pure nitrogen atmosphere in gas chromatography vaporization chamber and reduction treating; and aging at 220-280 degrees C in high-purity nitrogen atmosphere for 0.5-2 hours. USE - Method for preparing functionalized graphene coated probe (claimed). ADVANTAGE - The method is simple at low cost. DETAILED DESCRIPTION - Preparation of functionalized graphene coated probe comprises treating metal core front with acid, washing and drying; converting to 3-aminopropyl-triethoxysilane; immersing in 0.1 wt.% graphite oxide at 60-80 degrees C for 1-3 hours and drying at room temperature for 6-8 hours; immersing in aqueous ammonia solution, reacting at 60-80 degrees C, washing, drying, reacting with acetyl chloride, washing and drying; repeating (3)-(4) steps 4-7 times until coating thickness is 50-100 mu m; aging in pure nitrogen atmosphere of gas chromatography vaporization chamber and reduction treating; and aging at 220-280 degrees C in high-purity nitrogen atmosphere for 0.5-2 hours.