• 专利标题:   Preparing platinum-based single-atom catalyst comprises dissolving graphene, cobalt-containing precursor powder and terephthalic acid organic ligand in alcoholic solvent 1, subjecting to precipitation, carry out microwave heating, adopting ultraviolet lamp to irradiate, drying and calcining.
  • 专利号:   CN116259771-A
  • 发明人:   ZHANG H, SHAO Z, HAO J
  • 专利权人:   CAS DALIAN CHEM PHYSICAL INST
  • 国际专利分类:   H01M004/88, H01M004/92
  • 专利详细信息:   CN116259771-A 13 Jun 2023 H01M-004/92 202356 Chinese
  • 申请详细信息:   CN116259771-A CN10192510 02 Mar 2023
  • 优先权号:   CN10192510

▎ 摘  要

NOVELTY - Preparing platinum-based single-atom catalyst comprises (i) dissolving graphene, cobalt-containing precursor powder, and terephthalic acid organic ligand in alcoholic solvent 1, stirring to obtain mixed solution 1, subjecting to precipitation and centrifugation, calcining to obtain MOF (Metal-organic frameworks) material doped with graphene; (ii) mixing Pt-based metal precursor solution and alcohol solvent II, and obtaining the mixed solution II after ultrasonication; (iii) carry out microwave heating of the mixed solution 2, adopting ultraviolet lamp to irradiate simultaneously, and obtaining the catalyst slurry that the MOF of graphene doping supports Pt single atom; and (iv) drying the catalyst slurry and calcining. USE - The catalyst is useful in the field of fuel cell oxygen reduction reaction (claimed). ADVANTAGE - The method improves the oxygen reduction ability of the catalyst.