• 专利标题:   Preparation of graphene powder comprises taking natural crystalline graphite flakes, carrying out Hummer method, dispersing, adding alkaline substance and organic solution, precipitating, filtering, heating, washing, and drying.
  • 专利号:   CN105712345-A
  • 发明人:   CAO Y, DU K, HU G, PENG Z, WU K
  • 专利权人:   UNIV CENT SOUTH
  • 国际专利分类:   C01B031/04
  • 专利详细信息:   CN105712345-A 29 Jun 2016 C01B-031/04 201660 Pages: 6 Chinese
  • 申请详细信息:   CN105712345-A CN10169418 23 Mar 2016
  • 优先权号:   CN10169418

▎ 摘  要

NOVELTY - Preparation of graphene powder comprises taking natural crystalline graphite flakes, carrying out Hummer method to obtain graphite oxide mother liquid, and ultrasonically dispersing; adding alkaline substance to neutralize solution, slowly adding organic solution, precipitating, and filtering, where alkaline substance is potassium hydroxide, sodium hydroxide and/or sodium carbonate and organic solution comprises 90-100 % organic solvent and 0-10% water; and high temperature heating at 500-700 degrees C under protection atmosphere, washing to remove impurities, and drying. USE - Method for preparing graphene powder (claimed). ADVANTAGE - The method has simple and easy operation process.